{"id":4507,"date":"2023-04-17T13:54:00","date_gmt":"2023-04-17T13:54:00","guid":{"rendered":"https:\/\/new.www.purdue.edu\/newsroom\/?p=4507"},"modified":"2024-08-20T12:55:45","modified_gmt":"2024-08-20T16:55:45","slug":"purdue-researchers-combine-electric-poling-and-3d-printing-into-a-single-step","status":"publish","type":"post","link":"https:\/\/www.purdue.edu\/newsroom\/2023\/Q2\/purdue-researchers-combine-electric-poling-and-3d-printing-into-a-single-step","title":{"rendered":"Purdue researchers combine electric poling and 3D printing into a single step"},"content":{"rendered":"<div class=\"purdue-initial-words-wrap\"><p class=\"purdue-initial-words\">WEST LAFAYETTE, Ind. &mdash;<\/p> \n<p>Manufacturers of smart medical devices, smart robots and other products with smart sensors could simplify their device design and fabrication using a patent-pending Purdue University method that combines piezoelectric poling of filament and 3D printing in a single process.<\/p>\n<\/div>\n\n\n<p>Traditional sensor materials have piezoelectric properties that make them suitable to create smart sensors. Applying stress in one direction produces voltage in another direction. Although these materials measure how much stress is applied, which is among the basic properties of sensors, they cannot be used in 3D printing.<\/p>\n\n\n\n<p>3D printing, also known as additive manufacturing, has several advantages over traditional manufacturing, including customizing parts\u2019 shapes and geometries beyond planar options. However, the polyvinylidene difluoride (PVdf) filament used in 3D printing doesn\u2019t have strong piezoelectric properties. Its dipoles are randomly oriented, which produces less voltage. As a result, traditional PVdf filament isn\u2019t a good indicator of stress, and electric poling must be conducted in a post-processing treatment, increasing time and cost.<\/p>\n\n\n\n<p>Purdue researchers in the&nbsp;<a href=\"https:\/\/polytechnic.purdue.edu\/\" rel=\"noreferrer noopener\" target=\"_blank\">Purdue Polytechnic Institute<\/a>&nbsp;have combined 3D printing and electric poling into a single process called electric poling-assisted additive manufacturing, or EPAM. It aligns the dipoles in PVdf filament during the print, which leads to a better indication of stress that is being applied. This allows 3D-printed parts to have both strong sensing abilities and customized shapes. Importantly, it saves time and money.<\/p>\n\n\n\n<p><a href=\"https:\/\/polytechnic.purdue.edu\/profile\/rnawroc\" rel=\"noreferrer noopener\" target=\"_blank\">Robert Nawrocki<\/a>, assistant professor in the&nbsp;<a href=\"https:\/\/polytechnic.purdue.edu\/schools\/engineering-technology\" rel=\"noreferrer noopener\" target=\"_blank\">School of Engineering Technology<\/a>&nbsp;in the Purdue Polytechnic Institute, said the EPAM process accomplishes stretching and poling simultaneously, which are necessary conditions for the polarization.<\/p>\n\n\n\n<p>\u201cDuring the EPAM process, stretching the molten PVdF rod rearranges the amorphous strands in the film plane, and the applied electric field aligns dipoles toward the same direction,\u201d Nawrocki said. \u201cThe EPAM process can print free-form PVdF structures and induce the formation of \u03b2-phase, which is primarily responsible for the piezoelectric response.\u201d<\/p>\n\n\n\n<p><a href=\"https:\/\/polytechnic.purdue.edu\/profile\/jmgarcia\" rel=\"noreferrer noopener\" target=\"_blank\">Jose M. Garcia-Bravo<\/a>&nbsp;and&nbsp;<a href=\"https:\/\/polytechnic.purdue.edu\/profile\/bnewell1\" rel=\"noreferrer noopener\" target=\"_blank\">Brittany Newell<\/a>, associate professors of in the School of Engineering Technology, Nawrocki and PhD candidate Jinsheng Fan successfully printed PVdf force sensors with a fused deposition modeling 3D printer with a corona electric poling setup.<\/p>\n\n\n\n<p>\u201cThe piezoelectric activity, measured in picocoulombs per newton, or pC\/N, was calculated based on the piezoelectric output voltage,\u201d Nawrocki said. \u201cThe average piezoelectric activity of EPAM-printed PVdF films was 47.76 pC\/N, or about five times higher than unpoled 3D-printed films, at 9.0 pC\/N. The piezoelectric activity of unpoled 3D-printed PVdF films indicated that 3D printing in the absence of an electric field did not result in dipole alignment.\u201d<\/p>\n\n\n\n<p>Nawrocki disclosed the innovation to the&nbsp;<a href=\"https:\/\/otc.prf.org\/\" rel=\"noreferrer noopener\" target=\"_blank\">Purdue Research Foundation Office of Technology Commercialization<\/a>, which has applied for patent protection on the intellectual property. Industry partners interested in further developing the technology should contact&nbsp;<a href=\"https:\/\/otc.prf.org\/staff\/dhananjay-sewak\/\" rel=\"noreferrer noopener\" target=\"_blank\">Dhananjay Sewak<\/a>,&nbsp;<a href=\"mailto:dsewak@prf.org\">dsewak@prf.org<\/a>, about&nbsp;<a href=\"https:\/\/inventions.prf.org\/innovation\/8473\" rel=\"noreferrer noopener\" target=\"_blank\">2022-NAWR-69857<\/a>.<\/p>\n\n\n\n<p>The next steps to commercialize the EPAM method are to build a single 3D printing machine that can print all of the sensor components, including live-poled PVdF, electrodes and also the structure.<\/p>\n\n\n\n<p>The research was published in the&nbsp;<a href=\"https:\/\/onlinelibrary.wiley.com\/doi\/full\/10.1002\/adem.202200485\" rel=\"noreferrer noopener\" target=\"_blank\">July 2022 issue of Advanced Engineering Materials<\/a>&nbsp;and the&nbsp;<a href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S2214860422006376\" rel=\"noreferrer noopener\" target=\"_blank\">December 2022 issue of Additive Manufacturing<\/a>. Nawrocki and the research team received funding and other support from Purdue University.<\/p>\n\n\n\n<h2 class=\"wp-block-heading\"><strong>About Purdue University<\/strong><\/h2>\n\n\n\n<p>Purdue University is a top public research institution developing practical solutions to today\u2019s toughest challenges. Ranked in each of the last five years as one of the 10 Most Innovative universities in the United States by U.S. News &amp; World Report, Purdue delivers world-changing research and out-of-this-world discovery. Committed to hands-on and online, real-world learning, Purdue offers a transformative education to all. Committed to affordability and accessibility, Purdue has frozen tuition and most fees at 2012-13 levels, enabling more students than ever to graduate debt-free. See how Purdue never stops in the persistent pursuit of the next giant leap at&nbsp;<a href=\"https:\/\/stories.purdue.edu\/\" rel=\"noreferrer noopener\" target=\"_blank\">https:\/\/stories.purdue.edu<\/a>.&nbsp;<\/p>\n\n\n\n<h2 class=\"wp-block-heading\"><strong>About Purdue Research Foundation Office of Technology Commercialization<\/strong><\/h2>\n\n\n\n<p>The\u00a0<a href=\"https:\/\/otc.prf.org\/\" target=\"_blank\" rel=\"noreferrer noopener\">Purdue Research Foundation Office of Technology Commercialization<\/a>\u00a0operates one of the most comprehensive technology transfer programs among leading research universities in the U.S. Services provided by this office support the economic development initiatives of Purdue University and benefit the university\u2019s academic activities through commercializing, licensing and protecting Purdue intellectual property. In fiscal year 2021, the office reported 159 deals finalized with 236 technologies signed, 394 disclosures received and 187 issued U.S. patents. The office is managed by the Purdue Research Foundation, which received the 2019 Innovation and Economic Prosperity Universities Award for Place from the Association of Public and Land-grant Universities. In 2020, IPWatchdog Institute ranked Purdue third nationally in startup creation and in the top 20 for patents. The Purdue Research Foundation is a private, nonprofit foundation created to advance the mission of Purdue University. Contact\u00a0<a href=\"mailto:otcip@prf.org\">otcip@prf.org<\/a>\u00a0for more information.<\/p>\n\n\n<div id=\"note\" class=\"post-content__attribution \">\n    <div class=\"columns\"> \n                    <div class=\"column\"> \n                <p class=\"post-content__source\">\n                    <strong>Writer:<\/strong>\u00a0Steve Martin,\u00a0<a href=\"mailto:sgmartin@prf.org\">sgmartin@prf.org<\/a><br><strong>Media contact:<\/strong>\u00a0Robert Nawrocki,\u00a0<a href=\"mailto:rnawroc@purdue.edu\">rnawroc@purdue.edu<\/a>                <\/p>\n            <\/div>\n                    <\/div>\n<\/div>\n","protected":false},"excerpt":{"rendered":"<p>WEST LAFAYETTE, Ind. &mdash; Manufacturers of smart medical devices, smart robots and other products with smart sensors could simplify their device design and fabrication using a patent-pending Purdue University method that combines piezoelectric poling of filament and 3D printing in<\/p>\n","protected":false},"author":3,"featured_media":4508,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_acf_changed":false,"footnotes":""},"categories":[316,7],"tags":[],"department":[70,24],"source":[35],"purdue_today_topic":[66],"coauthors":[44],"class_list":["post-4507","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-prf","category-research-excellence","department-purdue-polytechnic-institute","department-research-foundation","source-purdue-research-foundation","purdue_today_topic-research"],"acf":[],"_links":{"self":[{"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/posts\/4507","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/users\/3"}],"replies":[{"embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/comments?post=4507"}],"version-history":[{"count":1,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/posts\/4507\/revisions"}],"predecessor-version":[{"id":4509,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/posts\/4507\/revisions\/4509"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/media\/4508"}],"wp:attachment":[{"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/media?parent=4507"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/categories?post=4507"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/tags?post=4507"},{"taxonomy":"department","embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/department?post=4507"},{"taxonomy":"source","embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/source?post=4507"},{"taxonomy":"purdue_today_topic","embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/purdue_today_topic?post=4507"},{"taxonomy":"author","embeddable":true,"href":"https:\/\/www.purdue.edu\/newsroom\/wp-json\/wp\/v2\/coauthors?post=4507"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}